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Synthesis and Identification of Phenyl Azochalcone & bis- azo – Chalcone Derivatives Derived from P-amino Acetophenone

    Zahraa Talib Ghlib Ahmed Abdul-Hassan Nihad Ismael Taha

Kirkuk University Journal-Scientific Studies, 2018, Volume 13, Issue 2, Pages 307-322
10.32894/kujss.2018.145896

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Abstract

This work involves the synthesis of different substituted amino-chalcones via claisen- schmidt condensation reaction between p-amino acetophenone and different aromatic substituted benzaldehydes. The second step involves the conversion of amino-chalcones to diazonium salt which were reacted with different phenolic compounds to give azo-chalcone . Some azo-chalcones containing acetyl group wrer prepared by reactingdiazonium salt with para-hydroxyacetophenone, and this gave bis- azo-chalcoe on reaction with substituted aromatic benzaldehyde.
The chemical structure of the synthesized compounds were confirmed on the basis of their spectral data (FTIR, 1HNMR, 13CNMR) and CHN analysis.
Keywords:
    Chalcone azo bisazo chalcone
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(2018). Synthesis and Identification of Phenyl Azochalcone & bis- azo – Chalcone Derivatives Derived from P-amino Acetophenone. Kirkuk University Journal-Scientific Studies, 13(2), 307-322. doi: 10.32894/kujss.2018.145896
Zahraa Talib Ghlib; Ahmed Abdul-Hassan; Nihad Ismael Taha. "Synthesis and Identification of Phenyl Azochalcone & bis- azo – Chalcone Derivatives Derived from P-amino Acetophenone". Kirkuk University Journal-Scientific Studies, 13, 2, 2018, 307-322. doi: 10.32894/kujss.2018.145896
(2018). 'Synthesis and Identification of Phenyl Azochalcone & bis- azo – Chalcone Derivatives Derived from P-amino Acetophenone', Kirkuk University Journal-Scientific Studies, 13(2), pp. 307-322. doi: 10.32894/kujss.2018.145896
Synthesis and Identification of Phenyl Azochalcone & bis- azo – Chalcone Derivatives Derived from P-amino Acetophenone. Kirkuk University Journal-Scientific Studies, 2018; 13(2): 307-322. doi: 10.32894/kujss.2018.145896
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