Kirkuk Journal of Science

Kirkuk Journal of Science

Synthesis and Spectroscopic Investigation of Some New Chalcones and their transformation to pyrazoline derivatives

Authors
Abstract
A series of a new chalcone derivatives (2a-i) containing benzyloxy moiety have been synthesized on the basis of base catalyzed claisen –Schmidt condensation in high yields from the reaction of the prepared starting material 3-(4-cholrobenzyloxy) paraldehyde (1)with different substituted acetophenones. The prepared chalcones were treated with hydrazine hydrate according to the Michael addition reaction to obtain new pyrazoline deivatives (3a-i). Finally the structures of the synthesized compounds were elucidated by using spectral methods such as; FT-IR, 1H-nm, 13C-nmr and 13C- Dept 135 spectra.
Keywords

Volume 7, Issue 1
Spring 2012
Page 50-66

  • Receive Date 01 June 2012
  • Revise Date 20 June 2012
  • Accept Date 25 June 2012