In this study, some of the new compounds have been synthesized including some of different Schiff bases (1-6) via the reaction of phenyl-1,4-diamine with substituted benzaldehyde in absolute ethanol and converted into derivatives of 1,3-oxazepine-4,7-dione (7-12) via ring closure reaction [2+5] of Schiff bases with maleic anhydride in dry benzene then the 1, 3- oxazepine -4, 7- compounds (7-12) were reacted with phenylhydrazine to produce 1,3-diazepine-4,7-dione (13-18). The prepared compounds were characterized by determination of melting point, FT-IR and UV-Visspectra, and some of the prepared compounds have been characterized by (1H-NMR& C.H.N.) techniques.
Salim Jasim,S . (2018). Synthesis and Characterization of Some Bis-1,3 Oxazepine - 4,7- dione and 1, 3 – Diazepine -4,7- dione Derivatives. Kirkuk Journal of Science, 13(2), 149-165. doi: 10.32894/kujss.2018.145725
MLA
Salim Jasim,S . "Synthesis and Characterization of Some Bis-1,3 Oxazepine - 4,7- dione and 1, 3 – Diazepine -4,7- dione Derivatives", Kirkuk Journal of Science, 13, 2, 2018, 149-165. doi: 10.32894/kujss.2018.145725
HARVARD
Salim Jasim S. (2018). 'Synthesis and Characterization of Some Bis-1,3 Oxazepine - 4,7- dione and 1, 3 – Diazepine -4,7- dione Derivatives', Kirkuk Journal of Science, 13(2), pp. 149-165. doi: 10.32894/kujss.2018.145725
CHICAGO
S Salim Jasim, "Synthesis and Characterization of Some Bis-1,3 Oxazepine - 4,7- dione and 1, 3 – Diazepine -4,7- dione Derivatives," Kirkuk Journal of Science, 13 2 (2018): 149-165, doi: 10.32894/kujss.2018.145725
VANCOUVER
Salim Jasim S. Synthesis and Characterization of Some Bis-1,3 Oxazepine - 4,7- dione and 1, 3 – Diazepine -4,7- dione Derivatives. Kirkuk J. Sci.. 2018;13(2):149-165. doi: 10.32894/kujss.2018.145725
